HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1464032Generated: October 31, 2026
2-Aminobiphenyl → 1-Isothiocyanato-2-phenylbenzene
https://huagongshe.com/reaction/1464032
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Aminobiphenyl | HCID 7015 | — |
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Solvent | Water | HCID 962 | — |
| Product | 1-Isothiocyanato-2-phenylbenzene | HCID 519659 | — |
Reaction Steps
A mixture of 2-aminobiphenyl (10.2 g), thiophosgene (10.4 g), dioxane (50 ml) and water (100 ml) was prepared with cooling in an ice bath. The temperature was raised to 30° C. and stirred for 3 hours at 30° C. to yield 2-biphenylylisothiocyanate as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05302720 |
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| Source dataset | uspto-grants-1994_04 |
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| ORD ID | ord-2cccb94890904c5bb3b50d93810f8a12 |
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| Source note | uspto-grants-1994_04 |
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