HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidinocarbonitrile → HCID 178504668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidinocarbonitrile | HCID 73736 | — |
| Reactant | 4'-(Methylsulfonyl)-[1,1'-biphenyl]-2-amine hydrochloride | HCID 19089270 | — |
| Solvent | M-Cresol | HCID 342 | — |
| Product | HCID 178504668 | HCID 178504668 | — |
Reaction Steps
A mixture of 2-amino-4'-methanesulphonylbiphenyl hydrochloride (2.3 g), N-cyanopiperidine (1.3 g) and m-cresol (10 ml) was heated at 90°-95° C. for 10 hours to give N-(4'-methanesulphonyl-2-biphenylyl)piperidine-1-carboxamidine (m.p. 128°-129° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-eafb3ef557c04c31b7b45b2140f0d308 |
| Source note | uspto-grants-1994_04 |