HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Morpholinecarbonitrile → HCID 178423713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Morpholinecarbonitrile | HCID 73738 | — |
| Reactant | 4-Methyl[1,1'-biphenyl]-2-amine--hydrogen chloride (1/1) | HCID 19089222 | — |
| Solvent | M-Cresol | HCID 342 | — |
| Product | HCID 178423713 | HCID 178423713 | — |
Reaction Steps
A mixture of 2-amino-4-methylbiphenyl hydrochloride (7.7 g) and 4-cyanomorpholine (5.9 g) in m-cresol (45 ml) was heated at 90°-95° C. for 15 hours to yield N-(4-methyl-2-biphenylyl)morpholine-4-carboxamidine (m.p. 154°-155° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-05da2ece5cf0427fb5a2b97bd7992940 |
| Source note | uspto-grants-1994_04 |