HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcyanamide → HCID 178424488, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcyanamide | HCID 15112 | — |
| Reactant | HCID 19089292 | HCID 19089292 | — |
| Solvent | M-Cresol | HCID 342 | — |
| Product | HCID 178424488 | HCID 178424488 | — |
Reaction Steps
A mixture of 2-amino-3-methylbiphenyl hydrochloride (2.65 g), N,N-dimethylcyanamide (1.3 g) and m-cresol (20 ml) was heated at 90°-95° C. for 18 hours to give N,N-dimethyl-N'-(3-methyl-2-biphenylyl)guanidine as a colourless solid (m.p. 144°-145° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-8c875439d9294bd7876d00cd9c123e4d |
| Source note | uspto-grants-1994_04 |