Dimethylcyanamide → HCID 178424492, compound

HRID 1464058Notes

Reaction equation

HRID 1464058 reaction equation
Cl.[NH2:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[CH:10]=1.[CH3:16][N:17]([CH3:20])[C:18]#[N:19]>C1C(O)=CC=CC=1C>[CH3:16][N:17]([CH3:20])[C:18]([NH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[C:9]1[CH:14]=[CH:13][CH:12]=[C:11]([CH3:15])[CH:10]=1)=[NH:19]

Participants

4

Reactant 2

HCID 15112DimethylcyanamideHCID 27598232-Amino-3'-methylbiphenyl hydrochloride

Product 1

HCID 178424492HCID 178424492, compound

Reagents, catalysts & solvents 1

HCID 342M-CresolSolvent

Conditions

Temperature
100 °C

Procedure

A mixture of 2-amino-3'-methylbiphenyl hydrochloride (1 g), N,N-dimethylcyanamide (0.67 ml) in m-cresol (1 ml) was heated at 100° C. for 3 hours to give N,N-dimethyl-N'-(3'-methyl-2-biphenylyl)guanidine (m.p. 116° C.) which was crystallised from hexane.

Sources & evidence

ORD record
ord-edad7aa982244479928e2ba708279ed6
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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