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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1464058Generated: November 3, 2026

Dimethylcyanamide → HCID 178424492, compound

https://huagongshe.com/reaction/1464058

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylcyanamideHCID 15112—
Reactant2-Amino-3'-methylbiphenyl hydrochlorideHCID 2759823—
SolventM-CresolHCID 342—
ProductHCID 178424492HCID 178424492—

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 2-amino-3'-methylbiphenyl hydrochloride (1 g), N,N-dimethylcyanamide (0.67 ml) in m-cresol (1 ml) was heated at 100° C. for 3 hours to give N,N-dimethyl-N'-(3'-methyl-2-biphenylyl)guanidine (m.p. 116° C.) which was crystallised from hexane.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05302720
Source datasetuspto-grants-1994_04
ORD IDord-edad7aa982244479928e2ba708279ed6
Source noteuspto-grants-1994_04