反应详情

温度

120 °C

A mixture of 3-methylthioiodobenzene (30 g), 2-nitrobromobenzene (24 g) and copper powder (23 g) was heated at 120° C. for 34 hours to yield a residue which was purified by chromatography on a silica column eluted with hexane to give 3'-methylthio-2-nitrobiphenyl (m.p. 42°-43° C.).

1. customto yield a residue which
2. customwas purified by chromatography on a silica column
3. washeluted with hexane