HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1464065Generated: October 26, 2026
1-Bromo-2-nitrobenzene → HCID 19089237, compound
https://huagongshe.com/reaction/1464065
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1-Bromo-2-nitrobenzene | HCID 11341 | — |
| Reactant | 3-Iodothioanisole | HCID 10705783 | — |
| Catalyst | Copper | HCID 23978 | — |
| Product | HCID 19089237 | HCID 19089237 | — |
Reaction Steps
A mixture of 3-methylthioiodobenzene (30 g), 2-nitrobromobenzene (24 g) and copper powder (23 g) was heated at 120° C. for 34 hours to yield a residue which was purified by chromatography on a silica column eluted with hexane to give 3'-methylthio-2-nitrobiphenyl (m.p. 42°-43° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05302720 |
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| Source dataset | uspto-grants-1994_04 |
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| ORD ID | ord-e007fcf492314eedb9499ae80300072c |
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| Source note | uspto-grants-1994_04 |
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