HuagongsheHuagongshe Chemistry Print Report · For research reference only
3'-Methylthio-2-nitrobiphenyl → 2-Amino-3'-methylthiobiphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3'-Methylthio-2-nitrobiphenyl | HCID 19089237 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-Amino-3'-methylthiobiphenyl | HCID 19089269 | — |
Reaction Steps
3'-Methylthio-2-nitrobiphenyl (8 g) was heated at 90°-95° C. for 5 hours with hydrated sodium sulphide (15.6 g) and ethanol (200 ml) to give 2-amino-3'-methylthiobiphenyl (m.p. 114°-115° C.) as a brown oil which was converted into its hydrochloride salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-dbede0d520eb45cca9c8ea4427d38c0d |
| Source note | uspto-grants-1994_04 |