HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylcyanamide → HCID 178503142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylcyanamide | HCID 15112 | — |
| Reactant | 2-Amino-3'-methylthiobiphenyl hydrochloride | HCID 19089299 | — |
| Solvent | M-Cresol | HCID 342 | — |
| Product | HCID 178503142 | HCID 178503142 | — |
Reaction Steps
A mixture of 2-amino-3'-methylthiobiphenyl hydrochloride (3.3 g), N,N-dimethylcyanamide (1.55 ml) and m-cresol (10 ml) was heated at 90°-95° C. for 14 hours to give N,N-dimethyl-N'-(3'-methylthio-2-biphenylyl)guanidine (m.p. 94°-95° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-6abb07d2ff204bb5901b5d52806b6fa5 |
| Source note | uspto-grants-1994_04 |