Benzoyl isothiocyanate → HCID 19089190, compound

HRID 1464071Notes

Reaction equation

HRID 1464071 reaction equation
[C:1]([N:9]=[C:10]=[S:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[NH2:12][C:13]1[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=1[C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>ClCCl>[C:1]([NH:9][C:10]([NH:12][C:13]1[C:18]([CH3:19])=[CH:17][CH:16]=[CH:15][C:14]=1[C:20]1[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=1)=[S:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 68284Benzoyl isothiocyanateHCID 6030842-amino-3-methylbiphenyl

Product 1

HCID 19089190HCID 19089190, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

A mixture of benzoylisothiocyanate (8.78 g), 2-amino-3-methylbiphenyl (9.85 g) and dichloromethane (75 ml) at ambient temperature for two hours gave N-benzoyl-N'-(3-methyl-2-biphenylyl)thiourea (m.p. 172°-173° C.).

Sources & evidence

ORD record
ord-a7ec013a0d254b20a4b43d2a84504bff
Source dataset
uspto-grants-1994_04
Patent number
US05302720

Reaction notes

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