HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → HCID 19089303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Lead diacetate trihydrate | HCID 22456 | — |
| Reactant | HCID 19089278 | HCID 19089278 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19089303 | HCID 19089303 | — |
Reaction Steps
A suspension of N-(4-fluoro-2-biphenylyl)thiourea (11 g) in water (70 ml) was reacted with a solution of potassium hydroxide (25.2 g) in water (70 ml). Lead acetate trihydrate (17 g) in water (70 ml) was added and the reaction mixture heated at 90°-95° C. for 40 minutes to give 4-fluoro-2-biphenylylcyanamide (m.p. 68°-70° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-d67ed5b83c43496bb37db8483acfc053 |
| Source note | uspto-grants-1994_04 |