HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N-(5-fluoro-2-biphenylyl)thiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Fluoro-2-biphenylylisothiocyanate | HCID 19089275 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(5-fluoro-2-biphenylyl)thiourea | HCID 19089310 | — |
Reaction Steps
Reaction of 5-fluoro-2-biphenylylisothiocyanate (9.3 g) in ethanol (40 ml) with 28% aqueous ammonia solution (80 ml) at ambient temperature for 24 hours gave N-(5-fluoro-2-biphenylyl)thiourea as a yellow solid (m.p. 188°-190° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-49ae6bb6666e4be4bac2137aae5eee5b |
| Source note | uspto-grants-1994_04 |