HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Hydroxide → 5-Fluoro-2-biphenylylcyanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Lead diacetate trihydrate | HCID 22456 | — |
| Reactant | N-(5-fluoro-2-biphenylyl)thiourea | HCID 19089310 | — |
| Solvent | Water | HCID 962 | — |
| Product | 5-Fluoro-2-biphenylylcyanamide | HCID 19089223 | — |
Reaction Steps
A suspension of N-(5-fluoro-2-biphenylyl)thiourea (8 g) in water (40 ml) was reacted with a solution of potassium hydroxide (18.2 g) in water (40 ml), and a solution of lead acetate trihydrate (12.3 g) in water (70 ml). The reaction mixture heated at 90°-95° C. for 1 hour to give 5-fluoro-2-biphenylylcyanamide as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-facaa8de4b9a44368ed1abe1408833f0 |
| Source note | uspto-grants-1994_04 |