HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylthio-2-nitrobiphenyl → 2-Amino-4-methylthiobiphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylthio-2-nitrobiphenyl | HCID 19089266 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2-Amino-4-methylthiobiphenyl | HCID 19089196 | — |
Reaction Steps
4-Methylthio-2-nitrobiphenyl (15 g) was reduced with hydrated stannous chloride (64 g) in ethylacetate (300 ml) at ambient temperature for 15 hours to give 2-amino-4-methylthiobiphenyl as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-3094334e8f5e42a299b78fe8a05e823d |
| Source note | uspto-grants-1994_04 |