HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidin-4-ol → HCID 178511981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidin-4-ol | HCID 79341 | — |
| Reactant | HCID 19089180 | HCID 19089180 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178511981 | HCID 178511981 | — |
Reaction Steps
A mixture of 4'-fluoro-2-biphenylylcyanamide (1 g) and 4-hydroxypiperidine (0.6 g) in ethanol (10 ml) was heated at 90°-95° C. for 3 hours to give N-(4'-fluoro-2-biphenylyl)-4-hydroxypiperidine-1-carboxamidine as a colourless solid (m.p. 132°-133° C.) which was recrystallised from ethylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-260915f8077b4aa793087977ec1a65eb |
| Source note | uspto-grants-1994_04 |