HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 15175521, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2'-Fluoro-[1,1'-biphenyl]-2-amine | HCID 15500927 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 15175521 | HCID 15175521 | — |
Reaction Steps
Reaction of 2-amino-2'-fluorobiphenyl (5 g) with benzoylisothiocyanate (4.4 g) in dichloromethane (120 ml) at ambient temperature for 8 hours gave N-benzoyl-N'-(2'-fluoro-2-biphenylyl)thiourea (m.p. 110°-111° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-e1b839cf6855413ebe9ac5a2c133e48c |
| Source note | uspto-grants-1994_04 |