HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 15175539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 3'-Fluoro-2-biphenylylisothiocyanate | HCID 19089300 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15175539 | HCID 15175539 | — |
Reaction Steps
Reaction of 3'-fluoro-2-biphenylylisothiocyanate (11.2 g) with ethanol (50 ml) with 28% aqueous ammonia solution (100 ml) for 24 hours at ambient temperature yielded N-(3'-fluoro-2-biphenylyl)thiourea (m.p. 157°-159° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-5d128c2e39734555b7f86bcb99153575 |
| Source note | uspto-grants-1994_04 |