HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 178481027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 19089315 | HCID 19089315 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 178481027 | HCID 178481027 | — |
Reaction Steps
A mixture of 3'-fluoro-2-biphenylylcyanamide (4.1 g) and N-methylpiperazine (1.9 g) in 1,2-dimethoxyethane (30 ml) was heated at 90°-95° C. for 4 hours to yield N-(3'-fluoro-2-biphenylyl)-4-methylpiperazine-1-carboxamidine (m.p. 117°-118° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-cd6f64d33bc84969a71921babcb6c919 |
| Source note | uspto-grants-1994_04 |