HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19089335, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 15669342 | HCID 15669342 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 19089335 | HCID 19089335 | 27.4% |
Reaction Steps
The procedure of Example 4B was followed with 5-ethyl-4-methyl-2-thiophenesulfonamide (1.5 g, 7.3 mmole), 3,4-dichlorophenyl isocyanate (1.38 g, 7.3 mmole), acetone (7 0 ml), 1H NaOH (7.3 ml), concentrated HCl to give the named product as a white solid (2.17 g, 5 2 mmole).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302724 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-38293deeaa6e42d1a3d99b34f5d2889f |
| Source note | uspto-grants-1994_04 |