HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Methyl 2-(4-hydroxy-3-isobutylphenyl)-2-cyclopentyl-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methyl 2-(4-hydroxy-3-methallylphenyl)-2-cyclopentyl-acetate | HCID 19087784 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Methyl 2-(4-hydroxy-3-isobutylphenyl)-2-cyclopentyl-acetate | HCID 19087789 | — |
Reaction Steps
4 g (0.014 mol) of the compound from Example V are dissolved in 30 ml of methanol and 10 ml of acetic acid and hydrogenated at 5.3 bar using Pd/C as a catalyst. Reaction time: 2.5 h. After filtering off the catalyst, the solvent is evaporated in vacuo and a slightly yellowish oil is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304563 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-66e241d1bdb44173a4f185149c2bb8a9 |
| Source note | uspto-grants-1994_04 |