HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19087769, compound → HCID 19087766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19087769 | HCID 19087769 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19087766 | HCID 19087766 | — |
Reaction Steps
5.6 g (20 mmol) of the compound from Example XI are hydrogenated at 4 atm. in 100 ml of ethanol with the addition of 0.5 g of palladium/carbon (10% strength). The catalyst is filtered off with suction, the filtrate is concentrated and the residue is further reacted without further purification (quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304563 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-b6e484a6a5b64c9893df79ea5da5be36 |
| Source note | uspto-grants-1994_04 |