Sodium Hydroxide → HCID 57314186, compound

HRID 1464389Notes

Reaction equation

HRID 1464389 reaction equation
[N:1]1([C:6]2[CH:7]=[C:8]([CH2:24][C:25]([O:27]C)=[O:26])[CH:9]=[CH:10][C:11]=2[O:12][CH2:13][C:14]2[CH:23]=[CH:22][C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[N:15]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1.[OH-].[Na+]>C(O)(C)C>[N:1]1([C:6]2[CH:7]=[C:8]([CH2:24][C:25]([OH:27])=[O:26])[CH:9]=[CH:10][C:11]=2[O:12][CH2:13][C:14]2[CH:23]=[CH:22][C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[N:15]=2)[CH:5]=[CH:4][CH:3]=[CH:2]1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 57042027HCID 57042027, compound

Product 1

HCID 57314186HCID 57314186, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

In analogy to the procedure of Example XV, the title compound is prepared from 0.8 g (2 mmol) of the compound from Example XXX and 0.2 g (5 mmol) of sodium hydroxide in 50 ml of isopropanol.

Sources & evidence

ORD record
ord-dd4985bc909c42c3a3d764307fcf4bc4
Source dataset
uspto-grants-1994_04
Patent number
US05304563

Reaction notes

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