HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4,5,6,7-Tetrahydro-1-benzothiophene-2-carboxylic acid | HCID 2063443 | — |
| Product | 4,5,6,7-Tetrahydro-benzo[b]thiophene-2-carbonyl chloride | HCID 6485362 | — |
Reaction Steps
1.0 g of 4,5,6,7-tetrahydrobenzo[b]thiophene-2-carboxylic acid was reacted with 4 ml of thionyl chloride for 3.5 hours under reflux. Then, excess thionyl chloride was distilled off under reduced pressure to obtain 4,5,6,7-tetrahydrobenzo[b]thiophene-2-carbonyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304657 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-7fb9e1d23fca47a89f28e5f5c3d7c586 |
| Source note | uspto-grants-1994_04 |