HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenol → 1-Bromo-4-(methoxymethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenol | HCID 7808 | — |
| Reactant | Dimethoxymethane | HCID 8020 | — |
| Product | 1-Bromo-4-(methoxymethoxy)benzene | HCID 10465919 | 49% |
Reaction Steps
4-Methoxymethoxy-1-bromobenzene was prepared from formaldehyde dimethyl acetal and 4-bromophenol by the method of Y. P. Yardley and H. Fletcher, Synthesis 1976. p. 244. The boiling point of this derivative is 54°-56° C. at 0.1 hPa, and the yield is 49% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05304667 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-8ea7403dc76c45fd89822a787cb3221b |
| Source note | uspto-grants-1994_04 |