HRID1464709

反应详情

EQUATION

反应方程式

HRID 1464709 的结构方程式

CONDITIONS

反应条件

温度
180 °C

PROCEDURE

实验过程

0.5 g of anhydrous aluminium chloride was added to 50 g of 2,4,6-trimethylphenyl chloroformate and the mixture was heated at 180° C. for 1.5 hours at normal pressure. The reaction mixture was then cooled and worked up as described in Example 1. 2,4,6-Trimethylchlorobenzene was obtained in a yield of 72%.

WORKUP

后处理

  1. temperatureThe reaction mixture was then cooled