HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → (E,E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-[3-(3-thienyl)-2-propenyloxymethyl]benzylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (E)-3-[3--(3-thienyl)-2-propenyloxymethyl]benzyl bromide | HCID 15227910 | — |
| Reactant | (E)-N-ethyl-6,6-dimethyl-2-hepten-4-ynylamine hydrochloride | HCID 19917114 | — |
| Reactant | 2-Hepten-4-ynylamine | HCID 54073361 | — |
| Product | (E,E)-N-ethyl-N-(6,6-dimethyl-2-hepten-4-ynyl)-3-[3-(3-thienyl)-2-propenyloxymethyl]benzylamine hydrochloride | HCID 19086952 | — |
Reaction Steps
Compounds of Examples 2 to 7 were obtained by s performing the same reaction as in Example 1 except that the corresponding bromomethyl or chloromethyl derivatives and/or 2-hepten-4-ynylamine derivatives were used instead of the starting compounds, (E)-3-[3--(3-thienyl)-2-propenyloxymethyl]benzyl bromide and/or (E)- N-ethyl-6,6-dimethyl-2-hepten-4-ynylamine hydrochloride, which were used in the above-mentioned reaction. ( When the reaction product was a free base, the hydrochloride producing step in the after-treatment was not included.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306728 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-0ddf1e414a384e679ed922e1f94f0e6a |
| Source note | uspto-grants-1994_04 |