HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydride → HCID 19917128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydride | HCID 166653 | — |
| Reactant | Lithium | HCID 3028194 | — |
| Reactant | HCID 19917015 | HCID 19917015 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19917128 | HCID 19917128 | 99.1% |
Reaction Steps
0.20 g of the resulting ester compound was dissolved in 5 ml of tetrahydrofuran, and reduced as in Referential Example 31 with 25 mg of lithium alminum hydride to give 0.18 g of the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306728 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-ed26bd89c5cd478c909657717874124e |
| Source note | uspto-grants-1994_04 |