HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 19917089, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19917140 | HCID 19917140 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19917089 | HCID 19917089 | 96.9% |
Reaction Steps
0.9 g of the resulting ether compound was dissolved in 10 ml of ethanol, and an aqueous solution(10 ml) of 1.44 g of sodium hydroxide was added. The mixture was refluxed for 4 hours, and then acetic acid was added to the solution to acidify it. The solvent was evaporated, and ethyl acetate and water were added. The organic layer separated was worked up in a customary manner to give 0.75 g of the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05306728 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-82be9b0547514634a10c0534d211a9a5 |
| Source note | uspto-grants-1994_04 |