HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vinyl chloroformate → HCID 59601719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vinyl chloroformate | HCID 78808 | — |
| Reactant | N-Methoxyprop-2-enamide | HCID 13531445 | — |
| Product | HCID 59601719 | HCID 59601719 | — |
Reaction Steps
The synthesis was carried out analogously to synthesis example 8 using N-methoxy-acrylamide and chloroformic acid vinyl ester. Purification by column chromatography on silica gel (PE:EE=9:1) yielded 1.6 g (91% of th.) of the title compound as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999323B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-5457b3292eac4bc197a3beacfcc105ba |
| Source note | uspto-grants-2015_04 |