HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malonic Acid → HCID 56929678, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malonic Acid | HCID 867 | — |
| Reactant | Lorcaserin | HCID 11658860 | — |
| Solvent | HCID 131732659 | HCID 131732659 | — |
| Product | HCID 56929678 | HCID 56929678 | — |
Reaction Steps
(R)-8-Chloro-1-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine malonate salt was prepared by addition of malonic acid (1 eq.) to a solution of (R)-8-chloro-1-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine in isopropyl acetate. (R)-8-Chloro-1-methyl-2,3,4,5-tetrahydro-1H-3-benzazepine malonate salt had an extrapolated melting onset temperature by DSC of about 143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999970B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-2953559423f94078844955018ca3de24 |
| Source note | uspto-grants-2015_04 |