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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1465020Generated: November 1, 2026

HCID 67328188, compound → HCID 67327584, compound

https://huagongshe.com/reaction/1465020

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 67328188HCID 67328188—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 67327584HCID 6732758416.9%

Reaction Steps

The compound (1 g, 3.0 mmol) obtained in Step 2 of Example 39 was added to methanol (15 mL) and Pd/C (200 mg), and stirred under H2 atmosphere for 14 hours at room temperature. The reaction mixture was filtered using Celite and concentrated to obtain the title compound (152 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08999973B2
Source datasetuspto-grants-2015_04
ORD IDord-355f9a94e3ea4d34a17ac85a6095e5dc
Source noteuspto-grants-2015_04