HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67328188, compound → HCID 67327584, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67328188 | HCID 67328188 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67327584 | HCID 67327584 | 16.9% |
Reaction Steps
The compound (1 g, 3.0 mmol) obtained in Step 2 of Example 39 was added to methanol (15 mL) and Pd/C (200 mg), and stirred under H2 atmosphere for 14 hours at room temperature. The reaction mixture was filtered using Celite and concentrated to obtain the title compound (152 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999973B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-355f9a94e3ea4d34a17ac85a6095e5dc |
| Source note | uspto-grants-2015_04 |