HRID1465028

反应详情

EQUATION

反应方程式

HRID 1465028 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

t-Butyl 4-methyl-3-nitrophenylcarbamate (7.6 g, 30.13 mmol) was dissolved in ethanol (167 mL) and subjected to a reaction under 50 psi H2 gas. The reaction mixture was stirred for 2 hours and then concentrated by filtering with Celite to obtain the title compound without further purification.

WORKUP

后处理

  1. customsubjected to a reaction under 50 psi H2 gas
  2. concentrationconcentrated
  3. filtrationby filtering with Celite