HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Ethyl 1-(4-fluorophenyl)-4-methoxy-pyrazole-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Ethyl 1-(4-fluorophenyl)-4-hydroxy-1H-pyrazole-3-carboxylate | HCID 730292 | — |
| Product | Ethyl 1-(4-fluorophenyl)-4-methoxy-pyrazole-3-carboxylate | HCID 66611500 | — |
Reaction Steps
E1 was prepared from D1 following the general procedure reported in Preparative Example 16 Step 2 using methyl iodide for the alkylation. MS (ES) C13H13FN2O3 requires: 264. Found: 265 (M+H)+ and 287 (M+Na)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999982B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-7ff40aef26c04777b8e32f8a756de766 |
| Source note | uspto-grants-2015_04 |