4-Methylphenylhydrazine monohydrochloride → HCID 68924309, compound

HRID 1465293Notes

Reaction equation

HRID 1465293 reaction equation
[NH2:1][CH:2]1[CH2:7][CH2:6][CH2:5][N:4]([C:8](=[O:12])[CH2:9][CH2:10]Br)[CH2:3]1.Cl.[CH3:14][C:15]1[CH:20]=[CH:19][C:18]([NH:21]N)=[CH:17][CH:16]=1.[CH3:23][N:24]1[CH2:29][CH2:28][C:27](=O)[CH2:26][CH2:25]1>C(N(CC)CC)C>[NH2:1][CH:2]1[CH2:7][CH2:6][CH2:5][N:4]([C:8](=[O:12])[CH2:9][CH2:10][N:21]2[C:18]3[CH:19]=[CH:20][C:15]([CH3:14])=[CH:16][C:17]=3[C:26]3[CH2:25][N:24]([CH3:23])[CH2:29][CH2:28][C:27]2=3)[CH2:3]1

Participants

5

Reactant 3

HCID 125044-Methylphenylhydrazine monohydrochlorideHCID 740491-Methyl-4-piperidoneHCID 68734714HCID 68734714, compound

Product 1

HCID 68924309HCID 68924309, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(3-aminopiperidin-1-yl)-3-bromopropan-1-one, 4-methylphenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone.

Sources & evidence

ORD record
ord-9c9808d3373841cbb9ce4e7f961c7b42
Source dataset
uspto-grants-2015_04
Patent number
US08999978B2

Reaction notes

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