4-Methylphenylhydrazine monohydrochloride → HCID 57875960, compound

HRID 1465295Notes

Reaction equation

HRID 1465295 reaction equation
Br[CH2:2][CH2:3][C:4]([N:6]1[CH2:11][CH2:10][CH:9]([C:12]([OH:14])=[O:13])[CH2:8][CH2:7]1)=[O:5].Cl.[CH3:16][C:17]1[CH:22]=[CH:21][C:20]([NH:23]N)=[CH:19][CH:18]=1.[CH3:25][N:26]1[CH2:31][CH2:30][C:29](=O)[CH2:28][CH2:27]1>C(N(CC)CC)C>[CH3:25][N:26]1[CH2:31][CH2:30][C:29]2[N:23]([CH2:2][CH2:3][C:4]([N:6]3[CH2:11][CH2:10][CH:9]([C:12]([OH:14])=[O:13])[CH2:8][CH2:7]3)=[O:5])[C:20]3[CH:19]=[CH:18][C:17]([CH3:16])=[CH:22][C:21]=3[C:28]=2[CH2:27]1

Participants

5

Reactant 3

HCID 125044-Methylphenylhydrazine monohydrochlorideHCID 740491-Methyl-4-piperidoneHCID 68735164HCID 68735164, compound

Product 1

HCID 57875960HCID 57875960, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(3-bromopropanoyl)piperidine-4-carboxylic acid, 4-methylphenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone.

Sources & evidence

ORD record
ord-3a23bbbb5d8443cfa50dba7b462f4a9a
Source dataset
uspto-grants-2015_04
Patent number
US08999978B2

Reaction notes

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