Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) → HCID 57875997, compound

HRID 1465302Notes

Reaction equation

HRID 1465302 reaction equation
Br[CH2:2][CH2:3][N:4]1[CH2:8][CH2:7][CH2:6][CH:5]1[CH3:9].Cl.[Cl:11][C:12]1[CH:17]=[CH:16][C:15]([NH:18]N)=[CH:14][CH:13]=1.[CH3:20][N:21]1[CH2:26][CH2:25][C:24](=O)[CH2:23][CH2:22]1>C(N(CC)CC)C>[Cl:11][C:12]1[CH:17]=[CH:16][C:15]2[N:18]([CH2:2][CH2:3][N:4]3[CH2:8][CH2:7][CH2:6][CH:5]3[CH3:9])[C:24]3[CH2:25][CH2:26][N:21]([CH3:20])[CH2:22][C:23]=3[C:14]=2[CH:13]=1

Participants

5

Reactant 3

HCID 71600Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1)HCID 740491-Methyl-4-piperidoneHCID 61288936HCID 61288936, compound

Product 1

HCID 57875997HCID 57875997, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(2-bromoethyl)-2-methylpyrrolidine, 4-chlorophenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone

Sources & evidence

ORD record
ord-b183f741fa694705b8984d85a98d1515
Source dataset
uspto-grants-2015_04
Patent number
US08999978B2

Reaction notes

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