Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1) → HCID 57875926, compound

HRID 1465371Notes

Reaction equation

HRID 1465371 reaction equation
Br[CH2:2][CH2:3][N:4]1[CH2:9][CH2:8][N:7]([CH3:10])[CH2:6][CH2:5]1.Cl.[Cl:12][C:13]1[CH:18]=[CH:17][C:16]([NH:19]N)=[CH:15][CH:14]=1.[CH3:21][N:22]1[CH2:27][CH2:26][C:25](=O)[CH2:24][CH2:23]1>C(N(CC)CC)C>[Cl:12][C:13]1[CH:18]=[CH:17][C:16]2[N:19]([CH2:2][CH2:3][N:4]3[CH2:9][CH2:8][N:7]([CH3:10])[CH2:6][CH2:5]3)[C:25]3[CH2:26][CH2:27][N:22]([CH3:21])[CH2:23][C:24]=3[C:15]=2[CH:14]=1

Participants

5

Reactant 3

HCID 71600Hydrazine, (4-chlorophenyl)-, hydrochloride (1:1)HCID 740491-Methyl-4-piperidoneHCID 29919993HCID 29919993, compound

Product 1

HCID 57875926HCID 57875926, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

The title compound is prepared by following Method 8 by using 1-(2-bromoethyl)-4-methylpiperazine, 4-chlorophenylhydrazine hydrochloride, triethylamine and N-methyl-4-piperidone

Sources & evidence

ORD record
ord-94021cb654784482a2ebac99f6ece4b2
Source dataset
uspto-grants-2015_04
Patent number
US08999978B2

Reaction notes

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