HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86651849, compound → HCID 67030757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86651849 | HCID 86651849 | — |
| Reactant | HCID 86651851 | HCID 86651851 | — |
| Product | HCID 67030757 | HCID 67030757 | 95.3% |
Reaction Steps
Production Example 108, step 4, {4-[(E)-2-carboxyvinyl]benzyl}(triphenyl)phosphonium bromide (503.9 mg, 1.001 mmol) and 5-(4-acetylpyridin-1-yl)pyridine-2-carbaldehyde (257.3 g, 1.103 mmol) were condensed to give (2E)-3-(4-{2-[5-(4-acetylpyridin-1-yl)pyridin-2-yl]vinyl}phenyl)prop-2-enoic acid (355.1 mg, yield 94.0%) as a pale-brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999989B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-d37310d4092946ecb0fbdcb47d4925bd |
| Source note | uspto-grants-2015_04 |