HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl carbazate → HCID 67030348, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl carbazate | HCID 70091 | — |
| Reactant | HCID 67031019 | HCID 67031019 | — |
| Product | HCID 67030348 | HCID 67030348 | 85% |
Reaction Steps
By a method similar to Production Example 118, step 3, 3-(4-{2-[5-(4-acetylpyridin-1-yl)pyridin-2-yl]ethyl}phenyl)propionic acid (267.2 mg, 0.700 mmol) and tert-butyl carbazate (559.9 mg, 4.237 mmol) were condensed to give tert-butyl 2-[3-(4-{2-[5-(4-acetylpyridin-1-yl)pyridin-2-yl]ethyl}phenyl)propanoyl]hydrazinecarboxylate (292.0 mg, yield 84.1%) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999989B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-960345bb97f6429786d6cbae47f1b000 |
| Source note | uspto-grants-2015_04 |