HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 56969446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 67517760 | HCID 67517760 | — |
| Product | HCID 56969446 | HCID 56969446 | — |
Reaction Steps
To 2-(8-(2-Fluorobenzyl)-8-azabicyclo[3.2.1]octan-2-yl)-5-(3-(2-methylpyridin-4-yl)-1-trityl-1H-indazol-5-yl)-1,3,4-oxadiazole (40 mg, 0.054 mmol) 95% trifluoroacetic acid (3 mL) was added. The reaction was stirred at room temperature for 30 minutes. After reaction completion, triethylsilane (0.1 mL) was added. The reaction was concentrated and submitted for prep LC/MS. A total of 6 mg of purified compound was retrieved.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999966B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-c798e4cbbf7c44fc8189388953f8e788 |
| Source note | uspto-grants-2015_04 |