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HRID1466063

反应详情

EQUATION

反应方程式

HRID 1466063 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：Cc1c(C(O)CN2CCN(C(=O)OC(C)(C)C)CC2=O)ccc2c1COC2=O
HCID89526106

未命名化合物

PRODUCTS

生成物

1
结构：Cc1c(C(O)CN2CCNCC2=O)ccc2c1COC2=O
HCID89533484

未命名化合物

PROCEDURE

实验过程

The product of Step A was treated with TFA to remove the Boc group. The crude material was dissolved in aqueous sodium bicarbonate, extracted with Chloroform-IPA (3:1) three times, dried over sodium sulfate and concentrated to furnish the title compound (free base). LC-MS (IE, m/z): 291 [M+1]+.

WORKUP

后处理

  1. customto remove the Boc group
  2. dissolutionThe crude material was dissolved in aqueous sodium bicarbonate
  3. extractionextracted with Chloroform-IPA (3:1) three times
  4. dry with materialdried over sodium sulfate
  5. concentrationconcentrated