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HRID1466124

反应详情

EQUATION

反应方程式

HRID 1466124 的结构方程式

REACTANTS

反应物

2
结构：O=C1CNCCN1CCc1ccc([N+](=O)[O-])cc1
HCID89524891

未命名化合物

结构：COC(=O)c1cc([N+](=O)[O-])ccc1CC=O
HCID89525047

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)c1cc([N+](=O)[O-])ccc1CCN1CCN(CCc2ccc([N+](=O)[O-])cc2)C(=O)C1
HCID89533490

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 1-[2-(4-Nitrophenyl)ethyl]piperazin-2-one and Methyl 5-nitro-2-(2-oxoethyl)benzoate following essentially the same procedure as Example 6. The product was purified by mass-directed reverse phase HPLC (AcCN-Water with 0.1% TFA). LC-MS (IE, m/z): 457 [M+1]+.

WORKUP

后处理

  1. customThe product was purified by mass-directed reverse phase HPLC (AcCN-Water with 0.1% TFA)