Potassium Carbonate → HCID 86695717, compound

HRID 1466400Notes

Reaction equation

HRID 1466400 reaction equation
Cl[C:2]1[N:6]([CH3:7])[N:5]=[C:4]([C:8]([F:11])([F:10])[F:9])[C:3]=1[CH:12]=[O:13].[F:14][C:15]([F:24])([F:23])[C:16]1[CH:21]=[CH:20][C:19]([OH:22])=[CH:18][CH:17]=1.C(=O)([O-])[O-:26].[K+].[K+]>>[CH3:7][N:6]1[C:2]([O:22][C:19]2[CH:18]=[CH:17][C:16]([C:15]([F:23])([F:24])[F:14])=[CH:21][CH:20]=2)=[C:3]([C:12]([OH:13])=[O:26])[C:4]([C:8]([F:11])([F:10])[F:9])=[N:5]1

Participants

4

Procedure

The title compound was prepared using 5-chloro-1-methyl-3-(trifluoromethyl)-1H-pyrazole-4-carbaldehyde and 4-(trifluoromethyl)phenol in the manner similar to the method in Production Example 1 above except potassium carbonate was used instead of potassium hydroxide.

Sources & evidence

ORD record
ord-799896475d01460583bf61c3dc735696
Source dataset
uspto-grants-2015_04
Patent number
US09000024B2

Reaction notes

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