HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 3-(2-Oxo-propylsulfanyl)-benzoic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-(2-Oxo-propylsulfanyl)-benzoic acid | HCID 66765083 | — |
| Product | 3-(2-Oxo-propylsulfanyl)-benzoic acid ethyl ester | HCID 66765101 | — |
Reaction Steps
3-(2-Oxo-propylsulfanyl)-benzoic acid from the previous reaction was dissolved in ethanol and a catalytic amount of conc. H2SO4 was added. The reaction was monitored by analytical TLC and when it was complete the reaction was concentrated to dryness and the resulting residue was purified via silica gel chromatography to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09000025B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-9d8e3d678b22485cadca128bc1209fc9 |
| Source note | uspto-grants-2015_04 |