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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1467149Generated: October 30, 2026

2-Cyclohexen-1-OL → HCID 66746549, compound

https://huagongshe.com/reaction/1467149

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Cyclohexen-1-OLHCID 13198—
Reactant2-Amino-6-fluorobenzonitrileHCID 522659—
ProductHCID 66746549HCID 66746549—

Reaction Steps

Prepared as in Example 22b from cyclohex-2-enol and 2-amino-6-fluorobenzonitrile as a colorless oil (78%). 1H NMR (400 MHz, CDCl3) δ 1.64 (m, 1H), 1.96 (m, 4H), 2.15 (m, 1H), 4.39 (s, 2H), 4.82 (m, 1H), 5.87 (m, 1H), 5.98 (m, 1H), 6.30 (d, 2H), 7.20 (t, 1H). MS 215 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09000054B2
Source datasetuspto-grants-2015_04
ORD IDord-82ad7127ee564026970d77a3a68323c1
Source noteuspto-grants-2015_04