HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Cyclohexen-1-OL → HCID 66746549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Cyclohexen-1-OL | HCID 13198 | — |
| Reactant | 2-Amino-6-fluorobenzonitrile | HCID 522659 | — |
| Product | HCID 66746549 | HCID 66746549 | — |
Reaction Steps
Prepared as in Example 22b from cyclohex-2-enol and 2-amino-6-fluorobenzonitrile as a colorless oil (78%). 1H NMR (400 MHz, CDCl3) δ 1.64 (m, 1H), 1.96 (m, 4H), 2.15 (m, 1H), 4.39 (s, 2H), 4.82 (m, 1H), 5.87 (m, 1H), 5.98 (m, 1H), 6.30 (d, 2H), 7.20 (t, 1H). MS 215 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09000054B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-82ad7127ee564026970d77a3a68323c1 |
| Source note | uspto-grants-2015_04 |