Ethyl Acetoacetate → HCID 86658231, compound

HRID 1467151Notes

Reaction equation

[C:1]([O:4][CH:5]1[CH2:10][CH2:9][CH2:8][CH:7]([O:11][C:12]2[CH:17]=[CH:16][CH:15]=[C:14]([NH2:18])[C:13]=2[C:19]#[N:20])[CH:6]1[O:21][C:22](=[O:24])[CH3:23])(=[O:3])[CH3:2].O=[C:26]([CH3:33])[CH2:27][C:28]([O:30][CH2:31][CH3:32])=[O:29]>>[C:1]([O:4][CH:5]1[CH2:10][CH2:9][CH2:8][CH:7]([O:11][C:12]2[CH:17]=[CH:16][CH:15]=[C:14]3[C:13]=2[C:19]([NH2:20])=[C:27]([C:28]([O:30][CH2:31][CH3:32])=[O:29])[C:26]([CH3:33])=[N:18]3)[CH:6]1[O:21][C:22](=[O:24])[CH3:23])(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 8868Ethyl Acetoacetate

HCID 86658232HCID 86658232, compound

Product 1

HCID 86658231HCID 86658231, compound

Procedure

Prepared as in Example 2a from 3-(3-amino-2-cyanophenoxy)cyclohexane-1,2-diyl diacetate (Example 133b) and ethyl 3-oxobutanoate as a pale yellow solid (32%). MS 445 (MH+).

Sources & evidence

ORD record: ord-fca16aba9fd94709b9a6833d37119b2e
Source dataset: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09000054B2

Reaction notes

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