4-Methoxybenzylamine → HCID 66747275, compound

HRID 1467240Notes

Reaction equation

[OH:1][CH2:2][C:3]([CH3:8])([CH3:7])[C:4]([OH:6])=O.[CH3:9][O:10][C:11]1[CH:18]=[CH:17][C:14]([CH2:15][NH2:16])=[CH:13][CH:12]=1>>[OH:1][CH2:2][C:3]([CH3:8])([CH3:7])[C:4]([NH:16][CH2:15][C:14]1[CH:17]=[CH:18][C:11]([O:10][CH3:9])=[CH:12][CH:13]=1)=[O:6]

Participants

Reactant 2

HCID 754524-Methoxybenzylamine

HCID 785483-Hydroxy-2,2-dimethylpropionic acid

Product 1

HCID 66747275HCID 66747275, compoundYield 97%

Procedure

Prepared as in Example 4c from 3-hydroxy-2,2-dimethylpropanoic acid and 4-methoxybenzylamine in 97% yield as a white solid. MS 238 (MH+).

Sources & evidence

ORD record: ord-5be780dfbe4a41169de18f7ba6e0508b
Source dataset: uspto-grants-2015_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09000054B2

Reaction notes

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