HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 56591357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86681280 | HCID 86681280 | — |
| Catalyst | Triethylsilane | HCID 12052 | — |
| Product | HCID 56591357 | HCID 56591357 | — |
Reaction Steps
Trifluoroacetic acid (1 mL) was added to tort-butyl 3-phenyl-5-(3-(pyridin-4-yl)-1-trityl-1H-indazole-5-carboxamido)piperidine-1-carboxylate (0.104 mmol). The reaction was stirred at room temperature for 30 minutes. Triethylsilane (1 drop) was added to the reaction and stirred for an additional 5 minutes. The reaction was concentrated in vacuo and purified using prep LC/MS.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08999957B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-3b542e20659e49e5ba72eeeb51aa4d3f |
| Source note | uspto-grants-2015_04 |