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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1467328Generated: November 2, 2026

Trifluoroacetic acid → HCID 56591357, compound

https://huagongshe.com/reaction/1467328

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 86681280HCID 86681280—
CatalystTriethylsilaneHCID 12052—
ProductHCID 56591357HCID 56591357—

Reaction Steps

Trifluoroacetic acid (1 mL) was added to tort-butyl 3-phenyl-5-(3-(pyridin-4-yl)-1-trityl-1H-indazole-5-carboxamido)piperidine-1-carboxylate (0.104 mmol). The reaction was stirred at room temperature for 30 minutes. Triethylsilane (1 drop) was added to the reaction and stirred for an additional 5 minutes. The reaction was concentrated in vacuo and purified using prep LC/MS.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08999957B2
Source datasetuspto-grants-2015_04
ORD IDord-3b542e20659e49e5ba72eeeb51aa4d3f
Source noteuspto-grants-2015_04