HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89499916, compound → HCID 43808402, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89499916 | HCID 89499916 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 43808402 | HCID 43808402 | — |
Reaction Steps
33A was hydrogenated at 55 psi in EtOH (20 mL) in the presence of PtO2 (30 mg). After 24 h, the reaction was filtered through Celite® and concentrated to afford 0.4 g of dark oil as desired product. MS (ESI) m/z: 231.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09000172B2 |
| Source dataset | uspto-grants-2015_04 |
| ORD ID | ord-35207ff0494943a885a84667cb689404 |
| Source note | uspto-grants-2015_04 |